Step-stool conformation of a cyclic Schiff base derived from ethylenediamine and heptane-2,4,6-trione: evidence for partial hydrolysis in metal coordination
Authors of publication
Ranaweera, Samantha A.; Bruno, Donnadieu; Henry, W. P.; White, Mark. G.
Journal of publication
Acta Crystallographica Section C
Year of publication
2022
Journal volume
78
Journal issue
6
a
6.9163 ± 0.0004 Å
b
12.5609 ± 0.0008 Å
c
19.9264 ± 0.0012 Å
α
90°
β
90°
γ
90°
Cell volume
1731.11 ± 0.18 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
4
Space group number
61
Hermann-Mauguin space group symbol
P b c a
Hall space group symbol
-P 2ac 2ab
Residual factor for all reflections
0.04
Residual factor for significantly intense reflections
0.0347
Weighted residual factors for significantly intense reflections
0.0899
Weighted residual factors for all reflections included in the refinement
0.0939
Goodness-of-fit parameter for all reflections included in the refinement