Syntheses and crystal structures of four 4-(4-meth-oxy-phen-yl)piperazin-1-ium salts: tri-fluoro-acetate, 2,3,4,5,6-penta-fluoro-benzoate, 4-iodo-benzoate, and a polymorph with 4-methyl-benzoate.
Authors of publication
Vinaya, ?; Basavaraju, Yeriyur B.; Yathirajan, Hemmige S.; Parkin, Sean
Journal of publication
Acta crystallographica. Section E, Crystallographic communications
Year of publication
2023
Journal volume
79
Journal issue
Pt 4
Pages of publication
380 - 385
a
16.2967 ± 0.0009 Å
b
6.0887 ± 0.0002 Å
c
28.4139 ± 0.0015 Å
α
90°
β
90°
γ
90°
Cell volume
2819.4 ± 0.2 Å3
Cell temperature
90 ± 0.2 K
Ambient diffraction temperature
90 ± 0.2 K
Number of distinct elements
5
Space group number
61
Hermann-Mauguin space group symbol
P b c a
Hall space group symbol
-P 2ac 2ab
Residual factor for all reflections
0.0403
Residual factor for significantly intense reflections
0.0336
Weighted residual factors for significantly intense reflections
0.0825
Weighted residual factors for all reflections included in the refinement
0.0871
Goodness-of-fit parameter for all reflections included in the refinement
