Information card for entry 2022740

Structure parameters

• Chemical name: Bis[4-(allyloxy)-<i>N</i>'-(but-2-en-1-ylidene)benzohydrazidato]nickel(II)
• Formula: C28 H30 N4 Ni O4
• Calculated formula: C28 H30 N4 Ni O4
• Title of publication: Crystal structure of bis-[4-(all-yloxy)-<i>N</i>'-(but-2-en-1-yl-idene)benzohydrazidato]nickel(II).
• Authors of publication: Khan, Sultana Shakila; Howlader, Md Belayet Hossain; Sheikh, Md Chanmiya; Miyatake, Ryuta; Zangrando, Ennio
• Journal of publication: Acta crystallographica. Section E, Crystallographic communications
• Year of publication: 2023
• Journal volume: 79
• Journal issue: Pt 5
• Pages of publication: 465 - 468
• a: 8.0978 ± 0.0008 Å
• b: 9.2021 ± 0.0009 Å
• c: 9.3316 ± 0.001 Å
• α: 84.027 ± 0.006°
• β: 88.091 ± 0.006°
• γ: 84.17 ± 0.006°
• Cell volume: 687.83 ± 0.12 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0471
• Residual factor for significantly intense reflections: 0.0395
• Weighted residual factors for significantly intense reflections: 0.0943
• Weighted residual factors for all reflections included in the refinement: 0.0979
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes