Information card for entry 2022842

Structure parameters

• Chemical name: (1,4,8,11-Tetraazacyclotetradecane-κ^4^<i>N</i>)nickel(II) tetraiodidocadmate(II)
• Formula: C10 H24 Cd I4 N4 Ni
• Calculated formula: C10 H24 Cd I4 N4 Ni
• Title of publication: Crystal structures of the complexes containing macrocyclic cations [M(cyclam)]2+ (M = Ni, Zn) and tetraiodidocadmate(2–) anion
• Authors of publication: Andriichuk, Irina L.; Shova, Sergiu; Lampeka, Yaroslaw D.
• Journal of publication: Acta Crystallographica Section E Crystallographic Communications
• Year of publication: 2023
• Journal volume: 79
• Journal issue: 9
• a: 15.4317 ± 0.0003 Å
• b: 17.2945 ± 0.0003 Å
• c: 7.98733 ± 0.00015 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2131.69 ± 0.07 ų
• Cell temperature: 199.95 ± 0.1 K
• Ambient diffraction temperature: 199.95 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0429
• Residual factor for significantly intense reflections: 0.0314
• Weighted residual factors for significantly intense reflections: 0.0586
• Weighted residual factors for all reflections included in the refinement: 0.0636
• Goodness-of-fit parameter for all reflections included in the refinement: 1.062
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes