Information card for entry 2022869

Structure parameters

• Chemical name: Bis(μ-2-methylpyridine <i>N</i>-oxide-κ^2^<i>O</i>:<i>O</i>)bis[dibromido(2-methylpyridine <i>N</i>-oxide-κ<i>O</i>)cobalt(II)] butanol monosolvate
• Formula: C28 H38 Br4 Co2 N4 O5
• Calculated formula: C28 H38 Br4 Co2 N4 O5
• Title of publication: Synthesis, crystal structure and reactivity of bis-(μ-2-methyl-pyridine <i>N</i>-oxide-κ²<i>O</i>:<i>O</i>)bis-[di-bromido-(2-methyl-pyridine <i>N</i>-oxide-κ<i>O</i>)cobalt(II)] butanol monosolvate.
• Authors of publication: Näther, Christian; Jess, Inke
• Journal of publication: Acta crystallographica. Section E, Crystallographic communications
• Year of publication: 2023
• Journal volume: 79
• Journal issue: Pt 11
• Pages of publication: 972 - 976
• a: 8.09 ± 0.0001 Å
• b: 9.5772 ± 0.0001 Å
• c: 12.24 ± 0.0001 Å
• α: 70.242 ± 0.001°
• β: 76.004 ± 0.001°
• γ: 83.86 ± 0.001°
• Cell volume: 865.693 ± 0.017 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0245
• Residual factor for significantly intense reflections: 0.0244
• Weighted residual factors for significantly intense reflections: 0.0648
• Weighted residual factors for all reflections included in the refinement: 0.0649
• Goodness-of-fit parameter for all reflections included in the refinement: 1.092
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes