Information card for entry 2022921

Structure parameters

• Chemical name: Poly[[μ-1,2-bis(pyridin-4-yl)ethene-κ^2^<i>N</i>:<i>N</i>'-μ-bromido-copper(I)] 1,2-bis(pyridin-4-yl)ethene 0.25-solvate]
• Formula: C15 H12.5 Br Cu N2.5
• Calculated formula: C15 H12.5 Br Cu N2.5
• Title of publication: Synthesis, crystal structure and thermal properties of poly[[μ-1,2-bis-(pyridin-4-yl)ethene-κ²<i>N</i>:<i>N</i>'-μ-bromido-copper(I)] 1,2-bis-(pyridin-4-yl)ethene 0.25-solvate].
• Authors of publication: Näther, Christian; Müller-Meinhard, Asmus; Jess, Inke
• Journal of publication: Acta crystallographica. Section E, Crystallographic communications
• Year of publication: 2023
• Journal volume: 79
• Journal issue: Pt 11
• Pages of publication: 1028 - 1032
• a: 7.7421 ± 0.0002 Å
• b: 10.1612 ± 0.0002 Å
• c: 10.1749 ± 0.0003 Å
• α: 72.143 ± 0.002°
• β: 73.252 ± 0.003°
• γ: 68.004 ± 0.002°
• Cell volume: 692.67 ± 0.03 ų
• Cell temperature: 100.1 ± 0.3 K
• Ambient diffraction temperature: 100.1 ± 0.3 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0296
• Residual factor for significantly intense reflections: 0.0293
• Weighted residual factors for significantly intense reflections: 0.0753
• Weighted residual factors for all reflections included in the refinement: 0.0755
• Goodness-of-fit parameter for all reflections included in the refinement: 1.085
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes