Information card for entry 2023238

Structure parameters

• Chemical name: (1,4,7,10,13,16-Hexaoxacyclooctadecane-1κ^6^<i>O</i>)(μ-oxalato-1κ^2^<i>O</i>^1^,<i>O</i>^2^:2κ^2^<i>O</i>^1'^,<i>O</i>^2'^)triphenyl-2κ^3^<i>C</i>-potassium(I)tin(IV)
• Formula: C32 H39 K O10 Sn
• Calculated formula: C32 H39 K O10 Sn
• Title of publication: Crystal structure of (1,4,7,10,13,16-hexaoxacyclooctadecane-κ6 O)potassium-μ-oxalato-triphenylstannate(IV), the first reported 18-crown-6-stabilized potassium salt of triphenyloxalatostannate
• Authors of publication: Song, Xueqing; Li, William; Torres, Yolanda; Greaves, Tazena
• Journal of publication: Acta Crystallographica Section E Crystallographic Communications
• Year of publication: 2024
• Journal volume: 80
• Journal issue: 9
• a: 9.406 ± 0.0003 Å
• b: 19.3779 ± 0.0004 Å
• c: 9.4225 ± 0.0003 Å
• α: 90°
• β: 97.925 ± 0.002°
• γ: 90°
• Cell volume: 1701.02 ± 0.08 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100.15 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0368
• Residual factor for significantly intense reflections: 0.0327
• Weighted residual factors for significantly intense reflections: 0.0848
• Weighted residual factors for all reflections included in the refinement: 0.1049
• Goodness-of-fit parameter for all reflections included in the refinement: 1.077
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No