Crystal Engineering Using Bisphenols. Chains, Ladders and Sheets Formed by the Adducts of 1,4-Diazabicyclo[2.2.2]octane with Bisphenols: Structures of Adducts with 4,4'-Isopropylidenediphenol (1/1), 4,4'-Oxodiphenol (1/1) and 4,4'-Thiodiphenol (1/1 and 2/1)
Authors of publication
Ferguson, George
Journal of publication
Acta Crystallographica Section B
Year of publication
1997
Journal volume
53
Journal issue
3
Pages of publication
513 - 520
a
9.4222 ± 0.0011 Å
b
11.1886 ± 0.0015 Å
c
15.694 ± 0.002 Å
α
90°
β
90°
γ
90°
Cell volume
1654.5 ± 0.4 Å3
Cell temperature
294 ± 1 K
Ambient diffraction temperature
294 ± 1 K
Number of distinct elements
4
Space group number
19
Hermann-Mauguin space group symbol
P 21 21 21
Hall space group symbol
P 2ac 2ab
Residual factor for all reflections
0.0981
Residual factor for significantly intense reflections
0.0582
Weighted residual factors for all reflections
0.134
Weighted residual factors for significantly intense reflections
0.1197
Goodness-of-fit parameter for all reflections
0.951
Goodness-of-fit parameter for significantly intense reflections