Information card for entry 2102693

Structure parameters

• Formula: C8 H16 I6 Pd S4
• Calculated formula: C8 H16 I6 Pd S4
• Title of publication: Extended structures of polyiodide salts of transition metal macrocyclic complexes
• Authors of publication: Blake, Alexander J.; Li, Wan-Sheung; Lippolis, Vito; Parsons, Simon; Schröder, Martin
• Journal of publication: Acta Crystallographica Section B
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 1
• Pages of publication: 81 - 92
• a: 18.062 ± 0.008 Å
• b: 23.602 ± 0.014 Å
• c: 11.166 ± 0.005 Å
• α: 90°
• β: 109.81 ± 0.06°
• γ: 90°
• Cell volume: 4478 ± 4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.049
• Residual factor for significantly intense reflections: 0.0404
• Weighted residual factors for significantly intense reflections: 0.0888
• Weighted residual factors for all reflections included in the refinement: 0.0931
• Goodness-of-fit parameter for all reflections included in the refinement: 1.23
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes