Structural studies on C-amidated amino acids and peptides: structures of hydrochloride salts of C-amidated Ile, Val, Thr, Ser, Met, Trp, Gln and Arg, and comparison with their C-unamidated counterparts
Authors of publication
In, Yasuko; Fujii, Mayumi; Sasada, Yasuhiro; Ishida, Toshimasa
Journal of publication
Acta Crystallographica Section B
Year of publication
2001
Journal volume
57
Journal issue
1
Pages of publication
72 - 81
a
7.6394 ± 0.0011 Å
b
5.2786 ± 0.0013 Å
c
14.5967 ± 0.0014 Å
α
90°
β
100.047 ± 0.01°
γ
90°
Cell volume
579.59 ± 0.18 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
5
Space group number
4
Hermann-Mauguin space group symbol
P 1 21 1
Hall space group symbol
P 2yb
Residual factor for all reflections
0.0307
Residual factor for significantly intense reflections
0.03
Weighted residual factors for all reflections included in the refinement
0.0945
Goodness-of-fit parameter for all reflections included in the refinement