Triphenylsilanol‒4,4'-bipyridyl (4/1), polymorph with Z' = 1
Formula
C82 H72 N2 O4 Si4
Calculated formula
C82 H72 N2 O4 Si4
Title of publication
The 1:1 adduct of triphenylsilanol and 4,4'-bipyridyl, and three pairwise-concomitant triclinic polymorphs of the 4:1 adduct having <i>Z</i>' = 0.5, 1 and 4
Authors of publication
Bowes, Katharine F.; Ferguson, George; Lough, Alan J.; Glidewell, Christopher
Journal of publication
Acta Crystallographica Section B
Year of publication
2003
Journal volume
59
Journal issue
2
Pages of publication
277 - 286
a
10.1595 ± 0.0019 Å
b
18.37 ± 0.004 Å
c
20.49 ± 0.004 Å
α
66.75 ± 0.03°
β
77.35 ± 0.03°
γ
80.95 ± 0.03°
Cell volume
3417.5 ± 1.4 Å3
Cell temperature
150 ± 1 K
Ambient diffraction temperature
150 ± 1 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.119
Residual factor for significantly intense reflections
0.0603
Weighted residual factors for significantly intense reflections
0.1522
Weighted residual factors for all reflections included in the refinement
0.1854
Goodness-of-fit parameter for all reflections included in the refinement
