Information card for entry 2104202

Structure parameters

• Formula: C18 H60 Cl18 P6 Sb4
• Calculated formula: C18 Cl18 P6 Sb4
• Title of publication: From six- to five-coordinated Sb^III^ in [(CH~3~)~3~PH]~3~[Sb~2~Cl~9~]: transition pathways from single-crystal X-ray diffraction
• Authors of publication: Gagor, Anna; Wojtaś, Maciej; Pietraszko, Adam; Jakubas, Ryszard
• Journal of publication: Acta Crystallographica Section B
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 5
• Pages of publication: 558 - 566
• a: 9.191 ± 0.0013 Å
• b: 9.191 ± 0.0013 Å
• c: 22.011 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 1610.3 ± 0.4 ų
• Cell temperature: 382 ± 2 K
• Ambient diffraction temperature: 382 ± 2 K
• Number of distinct elements: 5
• Space group number: 194
• Hermann-Mauguin space group symbol: P 63/m m c
• Hall space group symbol: -P 6c 2c
• Residual factor for all reflections: 0.1046
• Residual factor for significantly intense reflections: 0.0526
• Weighted residual factors for significantly intense reflections: 0.1426
• Weighted residual factors for all reflections included in the refinement: 0.169
• Goodness-of-fit parameter for all reflections included in the refinement: 0.993
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes