Syntheses, spectroscopic study and X-ray crystallography of some new phosphoramidates and lanthanide(III) complexes of <i>N</i>-(4-nitrobenzoyl)-<i>N</i>',<i>N</i>''-bis(morpholino)phosphoric triamide
Authors of publication
Gholivand, Khodayar; Mostaanzadeh, Hossein; Koval, Tomas; Dusek, Michal; Erben, Mauricio F.; Stoeckli-Evans, Helen; Della Védova, Carlos O.
Journal of publication
Acta Crystallographica Section B
Year of publication
2010
Journal volume
66
Journal issue
4
Pages of publication
441 - 450
a
16.2973 ± 0.0012 Å
b
11.1318 ± 0.0008 Å
c
9.4354 ± 0.0007 Å
α
90°
β
94.881 ± 0.002°
γ
90°
Cell volume
1705.5 ± 0.2 Å3
Cell temperature
120 ± 2 K
Ambient diffraction temperature
120 ± 2 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0659
Residual factor for significantly intense reflections
0.0487
Weighted residual factors for significantly intense reflections
0.1124
Weighted residual factors for all reflections included in the refinement
0.126
Goodness-of-fit parameter for all reflections included in the refinement
