Information card for entry 2105504

Structure parameters

• Formula: C24 H52.88 Mo N8 O14.44 Rh4
• Calculated formula: C24 H48 Mo N8 O14.436 Rh4
• Title of publication: Two- and three-dimensional assembled structures constructed from amidate-bridged paddlewheel complexes with group 6 oxometallate ions
• Authors of publication: Ebihara, Masahiro; Fuma, Yasuhiro
• Journal of publication: Acta Crystallographica Section B
• Year of publication: 2013
• Journal volume: 69
• Journal issue: 5
• Pages of publication: 480 - 489
• a: 12.952 ± 0.004 Å
• b: 13.849 ± 0.005 Å
• c: 14.679 ± 0.005 Å
• α: 112.46 ± 0.002°
• β: 99.574 ± 0.002°
• γ: 108.472 ± 0.003°
• Cell volume: 2180.4 ± 1.3 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0462
• Residual factor for significantly intense reflections: 0.0362
• Weighted residual factors for significantly intense reflections: 0.0746
• Weighted residual factors for all reflections included in the refinement: 0.0781
• Goodness-of-fit parameter for all reflections included in the refinement: 1.088
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No