Information card for entry 2108114

Structure parameters

• Formula: Cu0.966 Pb13.196 S24 Sb6.804
• Calculated formula: Cu0.956 Pb13.1548 S24 Sb6.8448
• Title of publication: Could incommensurability in sulfosalts be more common than thought? The case of meneghinite, CuPb~13~Sb~7~S~24~
• Authors of publication: Bindi, Luca; Petříček, Václav; Biagioni, Cristian; Plášil, Jakub; Moëlo, Yves
• Journal of publication: Acta Crystallographica Section B
• Year of publication: 2017
• Journal volume: 73
• Journal issue: 3
• Pages of publication: 369 - 376
• a: 24.0549 ± 0.0003 Å
• b: 4.1291 ± 0.0006 Å
• c: 11.3361 ± 0.0016 Å
• α: 90 ± 0.005°
• β: 90 ± 0.006°
• γ: 90 ± 0.005°
• Cell volume: 1126 ± 0.2 ų
• Cell temperature: 297.4 K
• Ambient diffraction temperature: 297.4 K
• Number of distinct elements: 4
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0682
• Residual factor for significantly intense reflections: 0.0479
• Weighted residual factors for significantly intense reflections: 0.1076
• Weighted residual factors for all reflections included in the refinement: 0.1145
• Goodness-of-fit parameter for significantly intense reflections: 2.21
• Goodness-of-fit parameter for all reflections included in the refinement: 1.97
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes