Crystallography Open Database

Information card for entry 2108900

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Structure parameters

Formula	C4 H15 O15 Rh
Calculated formula	C4 H15 O15 Rh
Title of publication	Oxonium <i>trans</i>-bis(oxalato)rhodate and related sodium salts: a rare example of crystalline complex acid
Authors of publication	Garkul, Ilia; Zadesenets, Andrey; Filatov, Evgeny; Baidina, Iraida; Tkachev, Sergey; Samsonenko, Denis; Korenev, Sergey
Journal of publication	Acta Crystallographica Section B
Year of publication	2021
Journal volume	77
Journal issue	6
Pages of publication	1048 - 1054
a	16.2131 ± 0.0008 Å
b	13.0362 ± 0.0006 Å
c	6.3015 ± 0.0003 Å
α	90°
β	99.572 ± 0.002°
γ	90°
Cell volume	1313.32 ± 0.11 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0313
Residual factor for significantly intense reflections	0.0277
Weighted residual factors for significantly intense reflections	0.0598
Weighted residual factors for all reflections included in the refinement	0.0618
Goodness-of-fit parameter for all reflections included in the refinement	1.069
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	Yes

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