Information card for entry 2200049

Structure parameters

• Common name: Bis[1,2-bis(diphenylphosphino)ethane-P,P'](dithioformato-S,S')technetium tris(benzene) solvate
• Formula: C71 H67 P4 S2 Tc
• Calculated formula: C71 H67 P4 S2 Tc
• Title of publication: Bis[1,2-bis(diphenylphosphino)ethane-<i>P</i>,<i>P</i>'](dithioformato-<i>S</i>,<i>S</i>')technetium tris(benzene) solvate
• Authors of publication: Bryan, Jeffrey C.; Burrell, Anthony K.; Kubas, Gregory J.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2001
• Journal volume: 57
• Journal issue: 1
• Pages of publication: m1 - m2
• a: 14.132 ± 0.004 Å
• b: 14.738 ± 0.006 Å
• c: 17.031 ± 0.004 Å
• α: 65.79 ± 0.03°
• β: 88.1 ± 0.03°
• γ: 67.88 ± 0.03°
• Cell volume: 2966 ± 2 ų
• Cell temperature: 193 K
• Ambient diffraction temperature: 193 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.066
• Residual factor for significantly intense reflections: 0.035
• Weighted residual factors for all reflections included in the refinement: 0.104
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes