Information card for entry 2200052

Structure parameters

• Chemical name: [(1RS,4RS)-5,5,7,13,15,15-Hexamethyl-1,4,8,12-tetraazacyclopentadeca- 7,12-diene-N^1^,N^4^,N^8^,N^12^]nickel(II) diperchlorate
• Formula: C17 H34 Cl2 N4 Ni O8
• Calculated formula: C17 H34 Cl2 N4 Ni O8
• Title of publication: [(1<i>RS</i>,4<i>RS</i>)-5,5,7,13,15,15-Hexamethyl-1,4,8,12-tetraazacyclopentadeca-7,12-diene-<i>N</i>^1^,<i>N</i>^4^,<i>N</i>^8^,<i>N</i>^12^]nickel(II) diperchlorate
• Authors of publication: Curtis, Neil F.; Waters, Joyce M.; Rickard, Clifton E.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2001
• Journal volume: 57
• Journal issue: 1
• Pages of publication: m48 - m50
• a: 10.3529 ± 0.0001 Å
• b: 16.1128 ± 0.0001 Å
• c: 15.04 ± 0.0001 Å
• α: 90°
• β: 107.025 ± 0.001°
• γ: 90°
• Cell volume: 2398.94 ± 0.03 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.051
• Residual factor for significantly intense reflections: 0.042
• Weighted residual factors for all reflections: 0.112
• Weighted residual factors for all reflections included in the refinement: 0.105
• Goodness-of-fit parameter for all reflections: 1.044
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No