Information card for entry 2200790

Structure parameters

• Chemical name: Palladium, tetrakis[μ-(cyano-C:N)]tetrakis(pentafluorophenyl) tetrakis(triethylphosphine)tetra-, cyclo (9CI), ditoluene
• Formula: C66 H76 F20 N4 P4 Pd4
• Calculated formula: C66 H76 F20 N4 P4 Pd4
• Title of publication: Square [Pd~4~(μ-CN)~4~(C~6~F~5~)~4~(PEt~3~)~4~]·2C~6~H~5~CH~3~
• Authors of publication: Jonathan P. H. Charmant; Pablo Espinet; Katerina Soulantica
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2001
• Journal volume: 57
• Journal issue: 10
• Pages of publication: m451 - m453
• a: 11.8845 ± 0.001 Å
• b: 14.8554 ± 0.0018 Å
• c: 21.652 ± 0.003 Å
• α: 90°
• β: 97.372 ± 0.009°
• γ: 90°
• Cell volume: 3791 ± 0.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.039
• Residual factor for significantly intense reflections: 0.025
• Weighted residual factors for all reflections included in the refinement: 0.061
• Goodness-of-fit parameter for all reflections included in the refinement: 0.97
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes