Information card for entry 2200858
Chemical name |
2,6,12,16-Tetraaza-1,7,11,17-tetraoxacycloicosane-diaquanickel(II) dichloride |
Formula |
C12 H32 Cl2 N4 Ni O6 |
Calculated formula |
C12 H32 Cl2 N4 Ni O6 |
Title of publication |
Further refinement of diaqua(1,7,11,17-tetraoxa-2,6,12,16-tetraazacycloeicosane-<i>N,N</i>',<i>N</i>'',<i>N</i>''')nickel(II) dichloride |
Authors of publication |
Kuksa, Vladimir A.; Wardell, Solange M. S. V; Lin, Paul Kong Thoo; Howie, R. Alan |
Journal of publication |
Acta Crystallographica Section E |
Year of publication |
2002 |
Journal volume |
58 |
Journal issue |
3 |
Pages of publication |
m74 - m76 |
a |
7.4288 ± 0.0003 Å |
b |
13.1426 ± 0.0005 Å |
c |
10.2527 ± 0.0003 Å |
α |
90° |
β |
102.248 ± 0.0018° |
γ |
90° |
Cell volume |
978.23 ± 0.06 Å3 |
Cell temperature |
150 ± 2 K |
Ambient diffraction temperature |
150 ± 2 K |
Number of distinct elements |
6 |
Space group number |
11 |
Hermann-Mauguin space group symbol |
P 1 21/m 1 |
Hall space group symbol |
-P 2yb |
Residual factor for all reflections |
0.0282 |
Residual factor for significantly intense reflections |
0.0246 |
Weighted residual factors for significantly intense reflections |
0.0613 |
Weighted residual factors for all reflections included in the refinement |
0.0631 |
Goodness-of-fit parameter for all reflections included in the refinement |
1.052 |
Diffraction radiation wavelength |
0.71073 Å |
Diffraction radiation type |
MoKα |
Has coordinates |
Yes |
Has disorder |
Yes |
Has Fobs |
Yes |
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The link is:
https://www.crystallography.net/2200858.html