Information card for entry 2200999

Structure parameters

• Formula: C32 H45.502 Cl4 Fe2 N8 O9.751
• Calculated formula: C32 H45.502 Cl4 Fe2 N8 O9.751
• Title of publication: μ-Oxo-bis{chloro[<i>N</i>,<i>N</i>'-dimethyl-<i>N</i>,<i>N</i>'-bis(2-pyridylmethyl)ethane-1,2-diamine]iron(III)} diperchlorate 0.751-hydrate
• Authors of publication: Rune Kirk Egdal; Alan Hazell; Christine J. McKenzie
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2002
• Journal volume: 58
• Journal issue: 1
• Pages of publication: m10 - m12
• a: 13.632 ± 0.003 Å
• b: 17.956 ± 0.004 Å
• c: 16.489 ± 0.003 Å
• α: 90°
• β: 94.938 ± 0.004°
• γ: 90°
• Cell volume: 4021.1 ± 1.5 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.032
• Weighted residual factors for all reflections included in the refinement: 0.034
• Goodness-of-fit parameter for all reflections included in the refinement: 0.88
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes