Information card for entry 2201276

Structure parameters

• Chemical name: Chloro-cis-dihydro-mer-tris(triphenylphosphine)rhodium(III) dichloromethane hemisolvate
• Formula: C54.5 H48 Cl2 P3 Rh
• Calculated formula: C54.5 H46 Cl2 P3 Rh
• Title of publication: Chloro-<i>cis</i>-dihydro-<i>mer</i>-tris(triphenylphosphine)rhodium(III) dichloromethane hemisolvate
• Authors of publication: Clegg, William; Elsegood, Mark R. J.; Norman, Nicholas C.; Pickett, Nigel L.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2002
• Journal volume: 58
• Journal issue: 8
• Pages of publication: m406 - m407
• a: 9.39 ± 0.005 Å
• b: 12.581 ± 0.006 Å
• c: 20.096 ± 0.01 Å
• α: 83.3 ± 0.05°
• β: 83.42 ± 0.04°
• γ: 76.64 ± 0.04°
• Cell volume: 2285 ± 2 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0663
• Residual factor for significantly intense reflections: 0.0385
• Weighted residual factors for significantly intense reflections: 0.098
• Weighted residual factors for all reflections included in the refinement: 0.109
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes