Information card for entry 2201297

Structure parameters

• Chemical name: bis(enneaaqualanthanum) vanadium octacosaoxide octahydrate
• Formula: H52 La2 O54 V10
• Calculated formula: H52 La2 O54 V10
• Title of publication: A novel polyoxometalate supramolecular compound: [La(H~2~O)~9~]~2~[V~10~O~28~]·8H~2~O
• Authors of publication: Peng, Xu-Hong; Li, Yi-Zhi; Cai, Li-Xiang; Wang, Liu-Fang; Wu, Ji-Gui
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2002
• Journal volume: 58
• Journal issue: 12
• Pages of publication: i111 - i113
• a: 9.818 ± 0.002 Å
• b: 11.935 ± 0.002 Å
• c: 19.514 ± 0.004 Å
• α: 90°
• β: 98.42 ± 0.03°
• γ: 90°
• Cell volume: 2262 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0442
• Residual factor for significantly intense reflections: 0.0393
• Weighted residual factors for significantly intense reflections: 0.1218
• Weighted residual factors for all reflections included in the refinement: 0.1236
• Goodness-of-fit parameter for all reflections included in the refinement: 1.073
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes