Information card for entry 2201478

Structure parameters

• Chemical name: undecacarbonyl-tri-μ-hydrido-(tricyclohexylphosphine)trirutheniumcobalt
• Formula: C29 H36 Co O11 P Ru3
• Calculated formula: C29 H36 Co O11 P Ru3
• Title of publication: A new heteronuclear trirutheniumcobalt cluster containing a bulky phosphine ligand, [CoRu~3~(μ-H)~3~(μ-CO)(CO)~10~(PCy~3~)]
• Authors of publication: Lozano Diz, Enrique; Therrien, Bruno; Süss-Fink, Georg
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2002
• Journal volume: 58
• Journal issue: 8
• Pages of publication: m451 - m453
• a: 9.6492 ± 0.0008 Å
• b: 16.4487 ± 0.0009 Å
• c: 21.6012 ± 0.0017 Å
• α: 90°
• β: 92.583 ± 0.01°
• γ: 90°
• Cell volume: 3425 ± 0.4 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0487
• Residual factor for significantly intense reflections: 0.0356
• Weighted residual factors for significantly intense reflections: 0.0865
• Weighted residual factors for all reflections included in the refinement: 0.0907
• Goodness-of-fit parameter for all reflections included in the refinement: 0.917
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes