Information card for entry 2201751

Structure parameters

• Chemical name: [(1-tert-Butyl-2-phenylvinylamino)(dimethylamino)dimethylsilyl-κ^2^N,N'] (N,N,N',N'-tetramethylenediamine-κ^2^N,N')lithium(I)
• Formula: C22 H43 Li N4 Si
• Calculated formula: C22 H43 Li N4 Si
• SMILES: [Li]12(N([Si]([N]1(C)C)(C)C)/C(=C\c1ccccc1)C(C)(C)C)[N](C)(C)CC[N]2(C)C
• Title of publication: [(1-<i>tert</i>-Butyl-2-phenylvinylamino)(dimethylamino)dimethylsilyl-κ^2^<i>N,N</i>'] (<i>N,N,N</i>',<i>N</i>'-tetramethylenediamine-κ^2^<i>N,N</i>')lithium(I)
• Authors of publication: He-Ping Shi; Dian-Sheng Liu; Shu-Ping Huang
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2003
• Journal volume: 59
• Journal issue: 6
• Pages of publication: m339 - m341
• a: 14.819 ± 0.003 Å
• b: 9.4142 ± 0.0016 Å
• c: 18.635 ± 0.003 Å
• α: 90°
• β: 97.674 ± 0.003°
• γ: 90°
• Cell volume: 2576.5 ± 0.8 ų
• Cell temperature: 178 ± 2 K
• Ambient diffraction temperature: 178 ± 2 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.1027
• Residual factor for significantly intense reflections: 0.0584
• Weighted residual factors for significantly intense reflections: 0.0582
• Weighted residual factors for all reflections included in the refinement: 0.0658
• Goodness-of-fit parameter for all reflections included in the refinement: 0.833
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes