Information card for entry 2202140

Structure parameters

• Chemical name: Bis{2-[(2-aminoethylimino)(phenyl)methyl]pyridine-κ^3^N}nickel(II) diperchlorate
• Formula: C30 H34 Cl2 N6 Ni O8
• Calculated formula: C30 H34 Cl2 N6 Ni O8
• SMILES: [Ni]1234([NH2]CCC[N]1=C(c1ccccc1)c1[n]2cccc1)[N](CCC[NH2]4)=C(c1ccccc1)c1[n]3cccc1.Cl(=O)(=O)(=O)[O-].Cl(=O)(=O)(=O)[O-]
• Title of publication: Bis{2-[(2-aminoethylimino)(phenyl)methyl]pyridine-κ^3^<i>N</i>}nickel(II) diperchlorate
• Authors of publication: Anwar Usman; Hoong-Kun Fun; Tapan K. Karmakar; Barindra K. Ghosh; Swapan K. Chandra
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2003
• Journal volume: 59
• Journal issue: 6
• Pages of publication: m387 - m389
• a: 10.0632 ± 0.0002 Å
• b: 16.5301 ± 0.0003 Å
• c: 10.2627 ± 0.0001 Å
• α: 90°
• β: 101.991 ± 0.001°
• γ: 90°
• Cell volume: 1669.91 ± 0.05 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0742
• Residual factor for significantly intense reflections: 0.0677
• Weighted residual factors for significantly intense reflections: 0.1923
• Weighted residual factors for all reflections included in the refinement: 0.1992
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes