Information card for entry 2202227

Structure parameters

• Chemical name: 4,11-Bis(4-chlorophenyl)-3,10-bis(2,6-dichlorophenyl)-1,8-dioxa-2,9- diazadispiro[4.1.4.2]trideca-2,9-dien-6-one chloroform methanol solvate
• Formula: C34.75 H24 Cl9 N2 O3.75
• Calculated formula: C34.75 H21 Cl9 N2 O3.75
• Title of publication: 4,11-Bis(4-chlorophenyl)-3,10-bis(2,6-dichlorophenyl)-1,8-dioxa-2,9-diazadispiro[4.1.4.2]trideca-2,9-dien-6-one‒chloroform‒methanol (1/1/0.75)
• Authors of publication: Li, Xiao-Fang; Feng, Ya-Qing; Hu Xiao-Fen
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2003
• Journal volume: 59
• Journal issue: 5
• Pages of publication: o670 - o671
• a: 9.896 ± 0.003 Å
• b: 14.724 ± 0.004 Å
• c: 15.55 ± 0.005 Å
• α: 111.815 ± 0.005°
• β: 101.814 ± 0.005°
• γ: 103.51 ± 0.005°
• Cell volume: 1935.7 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0869
• Residual factor for significantly intense reflections: 0.056
• Weighted residual factors for all reflections included in the refinement: 0.1954
• Goodness-of-fit parameter for all reflections included in the refinement: 1.095
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes