Information card for entry 2202305

Structure parameters

• Chemical name: 4,4'-bipyridinium(2+) di-μ-iodo-bis[(4,4'-bipyridyl)triiodobismuth(III)]
• Formula: C30 H26 Bi2 I8 N6
• Calculated formula: C30 H26 Bi2 I8 N6
• Title of publication: 4,4'-Bipyridyl adduct of an iodobismuthate anion linked by a 4,4'-bipyridinium cation
• Authors of publication: Jonathan P. H. Charmant; Nicholas C. Norman; A. Guy Orpen; Jonathan Starbuck
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2003
• Journal volume: 59
• Journal issue: 11
• Pages of publication: m1000 - m1001
• a: 9.6366 ± 0.0002 Å
• b: 12.7506 ± 0.0001 Å
• c: 18.1728 ± 0.0003 Å
• α: 90°
• β: 95.013 ± 0.001°
• γ: 90°
• Cell volume: 2224.39 ± 0.06 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0935
• Residual factor for significantly intense reflections: 0.0718
• Weighted residual factors for significantly intense reflections: 0.2002
• Weighted residual factors for all reflections included in the refinement: 0.2122
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes