Crystallography Open Database

Information card for entry 2202386

2202385 << 2202386 >> 2202387

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Structure parameters

Chemical name	Carbonyl[1-(2-pyridylmethyl)-1,4,7-triazacyclononane- κ^4^N](triphenylphosphine)ruthenium(II) dichloride dichloromethane sesquisolvate
Formula	C32.5 H38 Cl5 N4 O P Ru
Calculated formula	C32.5 H38 Cl5 N4 O P Ru
Title of publication	Carbonyl[1-(2-pyridylmethyl)-1,4,7-triazacyclononane-κ^4^<i>N</i>](triphenylphosphine)ruthenium(II) dichloride dichloromethane sesquisolvate
Authors of publication	Gott, Andrew L.; McGowan, Patrick C.; Thornton-Pett, Mark
Journal of publication	Acta Crystallographica Section E
Year of publication	2003
Journal volume	59
Journal issue	11
Pages of publication	m1015 - m1017
a	9.8492 ± 0.0002 Å
b	12.774 ± 0.0003 Å
c	16.0631 ± 0.0003 Å
α	74.5472 ± 0.0014°
β	75.3838 ± 0.0014°
γ	68.2566 ± 0.0009°
Cell volume	1782.47 ± 0.07 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0673
Residual factor for significantly intense reflections	0.0445
Weighted residual factors for significantly intense reflections	0.093
Weighted residual factors for all reflections included in the refinement	0.1051
Goodness-of-fit parameter for all reflections included in the refinement	1.081
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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