Crystallography Open Database

Information card for entry 2202667

2202666 << 2202667 >> 2202668

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Structure parameters

Formula	C24 H104 Co3 O68 V10
Calculated formula	C24 H96 Co3 O68 V10
Title of publication	A new decavanadate with a tricobalt(II) cation and 18-crown-6, tris{hexaaquacobalt(II)} decavanadate bis(18-crown-6) decahydrate
Authors of publication	Lee, Uk; Jung, Yeon-Hwa; Joo, Hea-Chung; Park, Ki-Min
Journal of publication	Acta Crystallographica Section E
Year of publication	2003
Journal volume	59
Journal issue	7
Pages of publication	m421 - m424
a	12.285 ± 0.004 Å
b	13.924 ± 0.003 Å
c	11.12 ± 0.003 Å
α	101.33 ± 0.03°
β	92.63 ± 0.02°
γ	84.26 ± 0.02°
Cell volume	1855.1 ± 0.9 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.066
Residual factor for significantly intense reflections	0.0419
Weighted residual factors for significantly intense reflections	0.0919
Weighted residual factors for all reflections included in the refinement	0.1077
Goodness-of-fit parameter for all reflections included in the refinement	1.084
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	Yes

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