Information card for entry 2202675

Structure parameters

• Chemical name: trans-Dichlorobis[ethane-1,2-diylbis(diphenylphophine)-κ2P,P']tungsten(II) hemipentane solvate
• Formula: C54.5 H54 Cl2 P4 W
• Calculated formula: C54.5 H54 Cl2 P4 W
• Title of publication: <i>trans</i>-Dichlorobis[ethane-1,2-diylbis(diphenylphophine)-κ^2^<i>P,P</i>']tungsten(II) pentane hemisolvate
• Authors of publication: Filippou, Alexander C.; Schnakenburg, Gregor; Philippopoulos, Athanassios I.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2003
• Journal volume: 59
• Journal issue: 8
• Pages of publication: m602 - m604
• a: 49.23 ± 0.013 Å
• b: 10.955 ± 0.002 Å
• c: 17.937 ± 0.004 Å
• α: 90°
• β: 99.49 ± 0.03°
• γ: 90°
• Cell volume: 9541 ± 4 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0473
• Residual factor for significantly intense reflections: 0.0357
• Weighted residual factors for significantly intense reflections: 0.0806
• Weighted residual factors for all reflections included in the refinement: 0.0837
• Goodness-of-fit parameter for all reflections included in the refinement: 0.954
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes