Information card for entry 2202729

Structure parameters

• Chemical name: (η^8^-Cyclooctatetraenyl)(2,2'',4,4'',6,6''-hexamethyl-μ- terphenyl-κC^2'^)(tetrahydrofuran-κO)thulium(III)
• Formula: C36 H41 O Tm
• Calculated formula: C36 H41 O Tm
• Title of publication: (η^8^-Cyclooctatetraene)(2,2'',4,4'',6,6''-hexamethyl-<i>m</i>-terphenyl-κ<i>C</i>^2'^)(tetrahydrofuran-κ<i>O</i>)thulium(III)
• Authors of publication: Rabe, Gerd W.; Zhang-Preße, Mei; Golen, James A.; Rheingold, Arnold L.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2003
• Journal volume: 59
• Journal issue: 12
• Pages of publication: m1102 - m1103
• a: 13.1317 ± 0.0009 Å
• b: 15.709 ± 0.001 Å
• c: 28.594 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5898.5 ± 0.7 ų
• Cell temperature: 218 ± 2 K
• Ambient diffraction temperature: 218 ± 2 K
• Number of distinct elements: 4
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0468
• Residual factor for significantly intense reflections: 0.0286
• Weighted residual factors for significantly intense reflections: 0.0641
• Weighted residual factors for all reflections included in the refinement: 0.072
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes