Information card for entry 2203067

Structure parameters

• Chemical name: Tetra-μ-alpha-isoleucine-bis[tetraaquasamarium(III)] hexaperchlorate
• Formula: C24 H68 Cl6 N4 O40 Sm2
• Calculated formula: C24 H52 Cl5.998 N4 O39.992 Sm2
• Title of publication: Tetra-μ-<small>L</small>-isoleucine-bis[tetraaquasamarium(III)] hexaperchlorate
• Authors of publication: Jinping Wang; Chunji Niu; Ninghai Hu; Jiazuan Ni
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2004
• Journal volume: 60
• Journal issue: 1
• Pages of publication: m32 - m34
• a: 21.682 ± 0.003 Å
• b: 10.3815 ± 0.0019 Å
• c: 15.177 ± 0.004 Å
• α: 90°
• β: 120.03 ± 0.03°
• γ: 90°
• Cell volume: 2957.6 ± 1.4 ų
• Cell temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for all reflections: 0.0571
• Residual factor for significantly intense reflections: 0.052
• Weighted residual factors for significantly intense reflections: 0.1354
• Weighted residual factors for all reflections included in the refinement: 0.1392
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes