Information card for entry 2203220

Structure parameters

• Chemical name: Bis[tris(2,2'-bipyridyl-κ^2^N,N')iron(II)] cyclo-tetravanadate decahydrate
• Formula: C60 H68 Fe2 N12 O22 V4
• Calculated formula: C60 H48 Fe2 N12 O22 V4
• Title of publication: Bis[tris(2,2'-bipyridyl-κ^2^<i>N,N</i>')iron(II)] <i>cyclo</i>-tetravanadate decahydrate
• Authors of publication: Ming-Hua Huang; Li-Hua Bi; Shao-Jun Dong
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2004
• Journal volume: 60
• Journal issue: 2
• Pages of publication: m153 - m155
• a: 21.619 ± 0.003 Å
• b: 13.656 ± 0.003 Å
• c: 23.517 ± 0.004 Å
• α: 90°
• β: 103.296 ± 0.014°
• γ: 90°
• Cell volume: 6757 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1116
• Residual factor for significantly intense reflections: 0.0741
• Weighted residual factors for significantly intense reflections: 0.195
• Weighted residual factors for all reflections included in the refinement: 0.2111
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes