Information card for entry 2203459

Structure parameters

• Chemical name: Bis(1,1,5,5-tetramethyl-2-thiobiuretato)nickel(II)
• Formula: C12 H24 N6 Ni O2 S2
• Calculated formula: C12 H24 N6 Ni O2 S2
• Title of publication: Bis(1,1,5,5-tetramethyl-2-thiobiuretato)nickel(II)
• Authors of publication: Jonathan D Crane; Matthew Whittingham
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2004
• Journal volume: 60
• Journal issue: 4
• Pages of publication: m449 - m451
• a: 13.935 ± 0.001 Å
• b: 7.0123 ± 0.0005 Å
• c: 18.4739 ± 0.0018 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1805.2 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0536
• Residual factor for significantly intense reflections: 0.0295
• Weighted residual factors for significantly intense reflections: 0.0556
• Weighted residual factors for all reflections included in the refinement: 0.0595
• Goodness-of-fit parameter for all reflections included in the refinement: 0.874
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes