Information card for entry 2203630

Structure parameters

• Chemical name: (1R,2R)-1,3-Bis(tert-butyldimethylsilyloxy)-2-(4-hydroxybutanamido)- 1-(4-nitrophenyl)propane
• Formula: C25 H46 N2 O6 Si2
• Calculated formula: C25 H46 N2 O6 Si2
• Title of publication: (1<i>R</i>,2<i>R</i>)-1,3-Bis(<i>tert</i>-butyldimethylsilyloxy)-2-(4-hydroxybutanamido)-1-(4-nitrophenyl)propane
• Authors of publication: Johansson, Dorte; Larsen, Frank B.; Bond, Andrew D.; Nielsen, Poul
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2004
• Journal volume: 60
• Journal issue: 5
• Pages of publication: o907 - o908
• a: 14.9014 ± 0.0012 Å
• b: 12.0241 ± 0.001 Å
• c: 17.2103 ± 0.0014 Å
• α: 90°
• β: 91.288 ± 0.002°
• γ: 90°
• Cell volume: 3082.9 ± 0.4 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.1012
• Residual factor for significantly intense reflections: 0.0564
• Weighted residual factors for significantly intense reflections: 0.1284
• Weighted residual factors for all reflections included in the refinement: 0.148
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes