Crystallography Open Database

Information card for entry 2203668

2203667 << 2203668 >> 2203669

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Structure parameters

Formula	C32 H64 Cu4 I6 K2 O16
Calculated formula	C32 H64 Cu4 I6 K2 O16
Title of publication	Bis[bis(12-crown-4)potassium] hexaiodotetracuprate(I)
Authors of publication	Heléne Paulsson; Andreas Fischer; Lars Kloo
Journal of publication	Acta Crystallographica Section E
Year of publication	2004
Journal volume	60
Journal issue	5
Pages of publication	m548 - m550
a	14.5859 ± 0.0001 Å
b	14.6371 ± 0.0001 Å
c	15.6526 ± 0.0002 Å
α	67.4428 ± 0.0005°
β	69.0664 ± 0.0004°
γ	64.1181 ± 0.0004°
Cell volume	2703.11 ± 0.04 Å³
Cell temperature	150 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0381
Residual factor for significantly intense reflections	0.027
Weighted residual factors for significantly intense reflections	0.0573
Weighted residual factors for all reflections included in the refinement	0.0614
Goodness-of-fit parameter for all reflections included in the refinement	1.032
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	Yes

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