Information card for entry 2204047

Structure parameters

• Common name: Tris-bis(trimethylsilyl)amido-samarium
• Chemical name: Tris[bis(trimethylsilyl)amido]samarium tetrahydrofuran solvate
• Formula: C22 H62 N3 O Si6 Sm
• Calculated formula: C22.08 H62.16 N3 O1.02 Si6 Sm
• Title of publication: Tris[bis(trimethylsilyl)amido]samarium tetrahydrofuran solvate
• Authors of publication: Jörg Sundermeyer; Alexandre Khvorost; Klaus Harms
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2004
• Journal volume: 60
• Journal issue: 8
• Pages of publication: m1117 - m1119
• a: 16.49 ± 0.003 Å
• b: 16.49 ± 0.003 Å
• c: 8.3485 ± 0.0011 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 1966 ± 0.6 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 163
• Hermann-Mauguin space group symbol: P -3 1 c
• Hall space group symbol: -P 3 2c
• Residual factor for all reflections: 0.0972
• Residual factor for significantly intense reflections: 0.0609
• Weighted residual factors for significantly intense reflections: 0.0949
• Weighted residual factors for all reflections included in the refinement: 0.1039
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes