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Information card for entry 2204328
Preview
Coordinates | 2204328.cif |
---|---|
Structure factors | 2204328.hkl |
Original IUCr paper | HTML |
Chemical name | [N,N'-bis(4-hydroxysalicylidene)-o-phenylenediamine]oxovanadium(IV) bis(dimethyl sulfoxide) dihydrate |
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Formula | C24 H30 N2 O9 S2 V |
Calculated formula | C24 H30 N2 O9 S2 V |
SMILES | [V]123([N](=Cc4c(O2)cc(O)cc4)c2ccccc2[N]1=Cc1ccc(O)cc1O3)=O.O=S(C)C.O=S(C)C.O.O |
Title of publication | A new Schiff base oxovanadium (IV) complex: [<i>N</i>,<i>N</i>'-bis(4-hydroxysalicylidene)-<i>o</i>-phenylenediamine]oxovanadium(IV) bis(dimethyl sulfoxide) dihydrate |
Authors of publication | Xie, Ming-Jin; Yan, Shi-Ping; Liao, Dai-Zheng; Jian, Zhong-Hui; Chen, Peng |
Journal of publication | Acta Crystallographica Section E |
Year of publication | 2004 |
Journal volume | 60 |
Journal issue | 10 |
Pages of publication | m1530 - m1532 |
a | 9.325 ± 0.003 Å |
b | 12.312 ± 0.004 Å |
c | 12.829 ± 0.004 Å |
α | 78.464 ± 0.005° |
β | 72.067 ± 0.006° |
γ | 85.072 ± 0.006° |
Cell volume | 1372.6 ± 0.8 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1314 |
Residual factor for significantly intense reflections | 0.0608 |
Weighted residual factors for significantly intense reflections | 0.1138 |
Weighted residual factors for all reflections included in the refinement | 0.1364 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.001 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | Yes |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/2204328.html
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