Information card for entry 2204579

Structure parameters

• Chemical name: Dilead pentaborate bromide
• Formula: B5 Br O9 Pb2
• Calculated formula: B5 Br O9 Pb2
• Title of publication: Reinvestigation of the Pb~2~[B~5~O~9~]Br structure based on single-crystal data
• Authors of publication: Yakubovich, Olga V.; Mochenova, Natalya N.; Dimitrova, Olga. V.; Massa, Werner
• Journal of publication: Acta Crystallographica, Section E
• Year of publication: 2004
• Journal volume: 60
• Journal issue: 11
• Pages of publication: i127 - i130
• a: 11.4935 ± 0.0019 Å
• b: 11.4717 ± 0.0019 Å
• c: 6.5297 ± 0.0011 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 860.9 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 34
• Hermann-Mauguin space group symbol: P n n 2
• Hall space group symbol: P 2 -2n
• Residual factor for all reflections: 0.0383
• Residual factor for significantly intense reflections: 0.0344
• Weighted residual factors for significantly intense reflections: 0.0776
• Weighted residual factors for all reflections included in the refinement: 0.0803
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No