Information card for entry 2204884

Structure parameters

• Chemical name: μ-4,4'-Di-4-pyridyldiazene-κ^2^N:N'- bis{[1,1,1-tris(diphenylphosphinomethyl)ethane-κP^3^]copper(I)} bis(tetrafluoroboride) dichloromethane solvate
• Formula: C93 H88 B2 Cl2 Cu2 F8 N4 P6
• Calculated formula: C93 H86 B2 Cl2 Cu2 F8 N4 P6
• Title of publication: μ-4,4'-Di-4-pyridyldiazene-κ^2^<i>N</i>:<i>N</i>'-bis{[1,1,1-tris(diphenylphosphinomethyl)ethane-κ<i>P</i>^3^]copper(I)} bis(tetrafluoroborate) dichloromethane solvate
• Authors of publication: Yu, Mingming; Li, Zhanxian; Fu, Wenfu; Zhang, Junfeng
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2005
• Journal volume: 61
• Journal issue: 1
• Pages of publication: m98 - m100
• a: 16.029 ± 0.011 Å
• b: 12.985 ± 0.009 Å
• c: 21.106 ± 0.014 Å
• α: 90°
• β: 103.768 ± 0.012°
• γ: 90°
• Cell volume: 4267 ± 5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0933
• Residual factor for significantly intense reflections: 0.0483
• Weighted residual factors for significantly intense reflections: 0.1227
• Weighted residual factors for all reflections included in the refinement: 0.1457
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No