Information card for entry 2205545

Structure parameters

• Chemical name: Tris(triphenylsilyl)phosphate dichloromethane solvate
• Formula: C54.26 H45.53 Cl0.53 O4 P Si3
• Calculated formula: C54.263 H45.526 Cl0.526 O4 P Si3
• Title of publication: Tris(triphenylsilyl)phosphate dichloromethane solvate
• Authors of publication: Ferguson, George; O'Leary, Brian J.; Spalding, Trevor R.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2005
• Journal volume: 61
• Journal issue: 4
• Pages of publication: o906 - o907
• a: 10.284 ± 0.002 Å
• b: 13.055 ± 0.003 Å
• c: 19.015 ± 0.004 Å
• α: 91.75 ± 0.02°
• β: 105.47 ± 0.02°
• γ: 106.31 ± 0.02°
• Cell volume: 2346 ± 0.9 ų
• Cell temperature: 294 ± 1 K
• Ambient diffraction temperature: 294 ± 1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1763
• Residual factor for significantly intense reflections: 0.0591
• Weighted residual factors for significantly intense reflections: 0.109
• Weighted residual factors for all reflections included in the refinement: 0.1304
• Goodness-of-fit parameter for all reflections included in the refinement: 0.856
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MolybdenumKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes