Information card for entry 2205906

Structure parameters

• Chemical name: Bis(dimethylformamide)-2κ^2^O-dipyridine-1κN,3κN-bis(μ-2'-salicylbenzohydrazidato)-1κ^4^O,N,N',O':2κ^2^N,O'';2κ^2^N,O'':3κ^4^O,N,N',O'-trinickel(II) dimethylformamide disolvate hemihydrate
• Formula: C50 H57 N10 Ni3 O10.5
• Calculated formula: C50 H57 N10 Ni3 O10.5
• Title of publication: Bis(dimethylformamide-2κ<i>O</i>)dipyridine-1κ<i>N</i>,3κ<i>N</i>-bis(μ-2'-salicylbenzohydrazidato)-1κ^3^<i>O</i>,<i>N</i>,<i>O</i>':2κ^2^<i>N</i>,<i>O</i>'';2κ^2^<i>N</i>,<i>O</i>'':3κ^3^<i>O</i>,<i>N</i>,<i>O</i>'-trinickel(II) dimethylformamide disolvate hemihydrate
• Authors of publication: Ming-Xing Yang; Shen Lin
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2005
• Journal volume: 61
• Journal issue: 6
• Pages of publication: m1095 - m1096
• a: 29.4926 ± 0.0015 Å
• b: 10.1678 ± 0.0003 Å
• c: 19.7293 ± 0.0003 Å
• α: 90°
• β: 115.389 ± 0.002°
• γ: 90°
• Cell volume: 5344.9 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0729
• Residual factor for significantly intense reflections: 0.0471
• Weighted residual factors for significantly intense reflections: 0.1245
• Weighted residual factors for all reflections included in the refinement: 0.1371
• Goodness-of-fit parameter for all reflections included in the refinement: 0.981
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes