A new nickel(II) complex [Ni<i>L</i>]·1.5CH~2~Cl~2~, where H~2~<i>L</i> is 14,25-dichloro-2,11-diphenyl-tetracyclo[20.4.0.0^4,9^.0^12,17^]hexacosa- 2,10,12,14,16,22,24,26-octaene-19,20-dione
Authors of publication
Rui-Hong Zhang; Guang-Ming Yang
Journal of publication
Acta Crystallographica Section E
Year of publication
2005
Journal volume
61
Journal issue
11
Pages of publication
m2434 - m2435
a
26.745 ± 0.007 Å
b
12.52 ± 0.003 Å
c
22.82 ± 0.006 Å
α
90°
β
118.454 ± 0.004°
γ
90°
Cell volume
6718 ± 3 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
6
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.0777
Residual factor for significantly intense reflections
0.0454
Weighted residual factors for significantly intense reflections
0.1082
Weighted residual factors for all reflections included in the refinement
0.1262
Goodness-of-fit parameter for all reflections included in the refinement
