Information card for entry 2207480

Structure parameters

• Chemical name: Tris(pyridine-kN)[salicylaldehyde (2-hydroxybenzoyl)hydrazonato-k^2^N,O]nickel(II) pyridine sesquisolvate
• Formula: C36.5 H32.5 N6.5 Ni O3
• Calculated formula: C36.5 H32.5 N6.5 Ni O3
• Title of publication: Tris(pyridine-κ<i>N</i>)[salicylaldehyde (2-hydroxybenzoyl)hydrazonato-κ^2^<i>N</i>,<i>O</i>]nickel(II) pyridine sesquisolvate
• Authors of publication: Zong-Qiu Hu; Wen-Hui Li; Yu Ding; Yu Wu
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2005
• Journal volume: 61
• Journal issue: 12
• Pages of publication: m2526 - m2527
• a: 12.5579 ± 0.001 Å
• b: 20.3993 ± 0.0017 Å
• c: 13.2756 ± 0.0011 Å
• α: 90°
• β: 93.493 ± 0.001°
• γ: 90°
• Cell volume: 3394.5 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0671
• Residual factor for significantly intense reflections: 0.0544
• Weighted residual factors for significantly intense reflections: 0.1451
• Weighted residual factors for all reflections included in the refinement: 0.1548
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes