Information card for entry 2207514

Structure parameters

• Chemical name: Bis{μ-dimethyl 1-[1-methoxycarbonyl-3-(methoxyoxalyl)-2-methylpropenyl]-3,3- dimethylcyclopropane-1,2- dicarboxylato(2-)}bis[(triphenylphosphine)palladium(II)] acetone solvate
• Formula: C75 H80 O19 P2 Pd2
• Calculated formula: C75 H80 O19 P2 Pd2
• Title of publication: Bis{μ-dimethyl 1-[1-methoxycarbonyl-3-(methoxyoxalyl)-2-methylpropenyl]-3,3-dimethylcyclopropane-1,2-dicarboxylato(2‒)}bis[(triphenylphosphine)palladium(II)] acetone solvate
• Authors of publication: Bolte, Michael; Rivas Nass, Andreas; Hashmi, A. Stephen K.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2005
• Journal volume: 61
• Journal issue: 12
• Pages of publication: m2677 - m2679
• a: 9.7819 ± 0.0003 Å
• b: 13.3852 ± 0.0003 Å
• c: 14.471 ± 0.0004 Å
• α: 98.446 ± 0.001°
• β: 102.79 ± 0.001°
• γ: 105.392 ± 0.001°
• Cell volume: 1738.31 ± 0.08 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.132
• Residual factor for significantly intense reflections: 0.0589
• Weighted residual factors for significantly intense reflections: 0.1267
• Weighted residual factors for all reflections included in the refinement: 0.1556
• Goodness-of-fit parameter for all reflections included in the refinement: 1.007
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes