Information card for entry 2207538

Structure parameters

• Chemical name: Tetra-μ-6-methylpyridin-2-olato-ditungsten toluene sesquisolvate
• Formula: C34.5 H36 N4 O4 W2
• Calculated formula: C34.5 H36 N4 O4 W2
• Title of publication: Tetra-μ-6-methylpyridin-2-olato-ditungsten toluene sesquisolvate
• Authors of publication: Chisholm, Malcolm H.; Gallucci, Judith C.; Hollandsworth, Carl B.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2005
• Journal volume: 61
• Journal issue: 12
• Pages of publication: m2503 - m2504
• a: 15.563 ± 0.002 Å
• b: 12.975 ± 0.002 Å
• c: 16.486 ± 0.003 Å
• α: 90°
• β: 96.48 ± 0.01°
• γ: 90°
• Cell volume: 3307.7 ± 0.9 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0563
• Residual factor for significantly intense reflections: 0.0344
• Weighted residual factors for significantly intense reflections: 0.0735
• Weighted residual factors for all reflections included in the refinement: 0.0805
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes