Information card for entry 2208290

Structure parameters

• Chemical name: bis[hexakis(N,N-dimethylacetamide)aluminium(III)] bis(N,N-dimethylacetamide)ium heptakis(perchlorate)
• Formula: C56 H127 Al2 Cl7 N14 O42
• Calculated formula: C56 H127 Al2 Cl7 N14 O42
• Title of publication: <i>N</i>,<i>N</i>-Dimethylacetamide complex of aluminium(III) perchlorate
• Authors of publication: Suzuki, Honoh; Ishiguro, Shin-ichi
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2006
• Journal volume: 62
• Journal issue: 3
• Pages of publication: m576 - m578
• a: 22.413 ± 0.002 Å
• b: 10.862 ± 0.002 Å
• c: 22.416 ± 0.003 Å
• α: 90°
• β: 118.8 ± 0.01°
• γ: 90°
• Cell volume: 4782.2 ± 1.3 ų
• Cell temperature: 297 ± 2 K
• Ambient diffraction temperature: 297 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1207
• Residual factor for significantly intense reflections: 0.0781
• Weighted residual factors for significantly intense reflections: 0.197
• Weighted residual factors for all reflections included in the refinement: 0.2443
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes