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Information card for entry 2208321
Preview
Coordinates | 2208321.cif |
---|---|
Structure factors | 2208321.hkl |
Original IUCr paper | HTML |
Chemical name | (diethyl ether)(μ~4~-2-{6-[1,3-dimethyl-3-(2-pyridyl)-1,4-bis(2,4,6- trimethylanilinio)butyl]-2-pyridyl}-2-methyl-1,3-bis(2,4,6- trimethylanilinio)propane)tetralithium(I) diethyl ether solvate |
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Formula | C59 H74 Li4 N6 O |
Calculated formula | C59 H74 Li4 N6 O |
Title of publication | Lithiation of the diaminopyridine protio-ligand MeC(2-C~5~H~4~N){CH~2~N(H)Mes}~2~ (Mes = 2,4,6-C~6~H~2~Me~3~) |
Authors of publication | Ward, Benjamin D.; Gade, Lutz H.; Mountford, Philip |
Journal of publication | Acta Crystallographica Section E |
Year of publication | 2006 |
Journal volume | 62 |
Journal issue | 3 |
Pages of publication | m472 - m474 |
a | 11.607 ± 0.002 Å |
b | 14.302 ± 0.003 Å |
c | 17.477 ± 0.004 Å |
α | 78.18 ± 0.03° |
β | 72.68 ± 0.03° |
γ | 80.31 ± 0.03° |
Cell volume | 2693 ± 1.1 Å3 |
Cell temperature | 173 K |
Ambient diffraction temperature | 173 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1479 |
Residual factor for significantly intense reflections | 0.0511 |
Weighted residual factors for all reflections | 0.1378 |
Weighted residual factors for significantly intense reflections | 0.0537 |
Weighted residual factors for all reflections included in the refinement | 0.0537 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.0869 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | Yes |
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