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Information card for entry 2209249
Preview
Coordinates | 2209249.cif |
---|---|
Structure factors | 2209249.hkl |
Original IUCr paper | HTML |
Common name | [(dppe)P 1+]2 [SnCl6 2-] . 2 CH2Cl2 |
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Chemical name | bis[1,1,3,3-tetraphenyl-1,3,2-triphospholenylium] hexachlorostannate dichloromethane solvate |
Formula | C54 H52 Cl10 P6 Sn |
Calculated formula | C54 H52 Cl10 P6 Sn |
SMILES | C1CP(=P[P+]1(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1.C(Cl)Cl.Cl[Sn](Cl)([Cl-])(Cl)(Cl)[Cl-].C1CP(=P[P+]1(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1.C(Cl)Cl |
Title of publication | Redetermination of a cyclic triphosphenium hexachlorostannate salt at 173 K |
Authors of publication | Ellis, Bobby D.; Macdonald, Charles L. B. |
Journal of publication | Acta Crystallographica Section E |
Year of publication | 2006 |
Journal volume | 62 |
Journal issue | 6 |
Pages of publication | m1235 - m1236 |
a | 10.8589 ± 0.0004 Å |
b | 11.5303 ± 0.0005 Å |
c | 13.0841 ± 0.0005 Å |
α | 68.777 ± 0.001° |
β | 79.774 ± 0.001° |
γ | 81.332 ± 0.001° |
Cell volume | 1496.16 ± 0.1 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0624 |
Residual factor for significantly intense reflections | 0.0539 |
Weighted residual factors for significantly intense reflections | 0.1015 |
Weighted residual factors for all reflections included in the refinement | 0.1121 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.234 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | Yes |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/2209249.html
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